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Beilstein J. Org. Chem. 2012, 8, 1909–1915, doi:10.3762/bjoc.8.221
Graphical Abstract
Scheme 1: Synthetic procedure for N,N''-dimethyldiethylene triamine.
Scheme 2: Standard reaction for the kinetic study.
Figure 1: Kinetic profile for varying [DMDETA].
Figure 2: Reaction order for copper from 0.025–0.64 mol %.
Figure 3: DMEDA versus DMDETA under air and nitrogen atmosphere.
Scheme 3: Long-chained aliphatic amines as ligands.